Preparation and Characterization of Polyaniline Nanotube

H. Shokry Hassan; M. F. Elkady; M. A. Abd El kawi; M. F. Alian

doi:doi:10.11648/j.ajac.s.2015030301.18

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Preparation and Characterization of Polyaniline Nanotube

H. Shokry Hassan, M. F. Elkady, M. A. Abd El kawi, M. F. Alian

Published in American Journal of Applied Chemistry (Volume 3, Issue 3-1)

Received: 30 April 2015 Accepted: 6 May 2015 Published: 13 May 2015

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Abstract

The present work reports slightly modification of the conventional chemical synthesis of polyaniline (PANI) to be nanotube structure without the need for any template or structural directing materials. PANI preparation was optimized by the oxidation of two different precursors: aniline and aniline hydrochloride with ammonium persulfate (APS) as oxidizing agent in various aqueous media of strong, weak acid and in alkaline medium at different pH values. Structural and morphological properties of the products are characterized by SEM, XRD and FTIR. Results showed the strong dependence of PANI nanotube on the acidity at certain pH value during the oxidation of aniline by APS. It is founded that, the optimum condition for preparation of PANI nanotube was obtained under oxidation of aniline monomer by APS in aqueous media of weak acid medium at pH five degree.

Published in	American Journal of Applied Chemistry (Volume 3, Issue 3-1) This article belongs to the Special Issue Nano-Technology for Environmental Aspects
DOI	10.11648/j.ajac.s.2015030301.18
Page(s)	54-59
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2015. Published by Science Publishing Group

Keywords

Characterization, Conducting Polymer, Polyaniline Nanotube

References

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APA Style

H. Shokry Hassan, M. F. Elkady, M. A. Abd El kawi, M. F. Alian. (2015). Preparation and Characterization of Polyaniline Nanotube. American Journal of Applied Chemistry, 3(3-1), 54-59. https://doi.org/10.11648/j.ajac.s.2015030301.18

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ACS Style

H. Shokry Hassan; M. F. Elkady; M. A. Abd El kawi; M. F. Alian. Preparation and Characterization of Polyaniline Nanotube. Am. J. Appl. Chem. 2015, 3(3-1), 54-59. doi: 10.11648/j.ajac.s.2015030301.18

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AMA Style

H. Shokry Hassan, M. F. Elkady, M. A. Abd El kawi, M. F. Alian. Preparation and Characterization of Polyaniline Nanotube. Am J Appl Chem. 2015;3(3-1):54-59. doi: 10.11648/j.ajac.s.2015030301.18

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@article{10.11648/j.ajac.s.2015030301.18,
  author = {H. Shokry Hassan and M. F. Elkady and M. A. Abd El kawi and M. F. Alian},
  title = {Preparation and Characterization of Polyaniline Nanotube},
  journal = {American Journal of Applied Chemistry},
  volume = {3},
  number = {3-1},
  pages = {54-59},
  doi = {10.11648/j.ajac.s.2015030301.18},
  url = {https://doi.org/10.11648/j.ajac.s.2015030301.18},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.s.2015030301.18},
  abstract = {The present work reports slightly modification of the conventional chemical synthesis of polyaniline (PANI) to be nanotube structure without the need for any template or structural directing materials. PANI preparation was optimized by the oxidation of two different precursors: aniline and aniline hydrochloride with ammonium persulfate (APS) as oxidizing agent in various aqueous media of strong, weak acid and in alkaline medium at different pH values. Structural and morphological properties of the products are characterized by SEM, XRD and FTIR. Results showed the strong dependence of PANI nanotube on the acidity at certain pH value during the oxidation of aniline by APS. It is founded that, the optimum condition for preparation of PANI nanotube was obtained under oxidation of aniline monomer by APS in aqueous media of weak acid medium at pH five degree.},
 year = {2015}
}

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TY  - JOUR
T1  - Preparation and Characterization of Polyaniline Nanotube
AU  - H. Shokry Hassan
AU  - M. F. Elkady
AU  - M. A. Abd El kawi
AU  - M. F. Alian
Y1  - 2015/05/13
PY  - 2015
N1  - https://doi.org/10.11648/j.ajac.s.2015030301.18
DO  - 10.11648/j.ajac.s.2015030301.18
T2  - American Journal of Applied Chemistry
JF  - American Journal of Applied Chemistry
JO  - American Journal of Applied Chemistry
SP  - 54
EP  - 59
PB  - Science Publishing Group
SN  - 2330-8745
UR  - https://doi.org/10.11648/j.ajac.s.2015030301.18
AB  - The present work reports slightly modification of the conventional chemical synthesis of polyaniline (PANI) to be nanotube structure without the need for any template or structural directing materials. PANI preparation was optimized by the oxidation of two different precursors: aniline and aniline hydrochloride with ammonium persulfate (APS) as oxidizing agent in various aqueous media of strong, weak acid and in alkaline medium at different pH values. Structural and morphological properties of the products are characterized by SEM, XRD and FTIR. Results showed the strong dependence of PANI nanotube on the acidity at certain pH value during the oxidation of aniline by APS. It is founded that, the optimum condition for preparation of PANI nanotube was obtained under oxidation of aniline monomer by APS in aqueous media of weak acid medium at pH five degree.
VL  - 3
IS  - 3-1
ER  -

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Author Information

H. Shokry Hassan

Electronic Materials Researches Department, Advanced Technology and New Materials and Research Institute (ATNMRI), City of Scientific Research and Technological Applications, Alexandria, Egypt
M. F. Elkady

Chemical and Petrochemical Engineering Department, Egypt-Japan University of Science and Technology, Alexandria, Egypt
M. A. Abd El kawi

Environmental Studies Department, Institute of Graduate Studies& Research, Alexandria University, Egypt
M. F. Alian

Environmental Studies Department, Institute of Graduate Studies& Research, Alexandria University, Egypt

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Plain Text BibTeX RIS

APA Style

H. Shokry Hassan, M. F. Elkady, M. A. Abd El kawi, M. F. Alian. (2015). Preparation and Characterization of Polyaniline Nanotube. American Journal of Applied Chemistry, 3(3-1), 54-59. https://doi.org/10.11648/j.ajac.s.2015030301.18

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ACS Style

H. Shokry Hassan; M. F. Elkady; M. A. Abd El kawi; M. F. Alian. Preparation and Characterization of Polyaniline Nanotube. Am. J. Appl. Chem. 2015, 3(3-1), 54-59. doi: 10.11648/j.ajac.s.2015030301.18

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AMA Style

H. Shokry Hassan, M. F. Elkady, M. A. Abd El kawi, M. F. Alian. Preparation and Characterization of Polyaniline Nanotube. Am J Appl Chem. 2015;3(3-1):54-59. doi: 10.11648/j.ajac.s.2015030301.18

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@article{10.11648/j.ajac.s.2015030301.18,
  author = {H. Shokry Hassan and M. F. Elkady and M. A. Abd El kawi and M. F. Alian},
  title = {Preparation and Characterization of Polyaniline Nanotube},
  journal = {American Journal of Applied Chemistry},
  volume = {3},
  number = {3-1},
  pages = {54-59},
  doi = {10.11648/j.ajac.s.2015030301.18},
  url = {https://doi.org/10.11648/j.ajac.s.2015030301.18},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.s.2015030301.18},
  abstract = {The present work reports slightly modification of the conventional chemical synthesis of polyaniline (PANI) to be nanotube structure without the need for any template or structural directing materials. PANI preparation was optimized by the oxidation of two different precursors: aniline and aniline hydrochloride with ammonium persulfate (APS) as oxidizing agent in various aqueous media of strong, weak acid and in alkaline medium at different pH values. Structural and morphological properties of the products are characterized by SEM, XRD and FTIR. Results showed the strong dependence of PANI nanotube on the acidity at certain pH value during the oxidation of aniline by APS. It is founded that, the optimum condition for preparation of PANI nanotube was obtained under oxidation of aniline monomer by APS in aqueous media of weak acid medium at pH five degree.},
 year = {2015}
}

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TY  - JOUR
T1  - Preparation and Characterization of Polyaniline Nanotube
AU  - H. Shokry Hassan
AU  - M. F. Elkady
AU  - M. A. Abd El kawi
AU  - M. F. Alian
Y1  - 2015/05/13
PY  - 2015
N1  - https://doi.org/10.11648/j.ajac.s.2015030301.18
DO  - 10.11648/j.ajac.s.2015030301.18
T2  - American Journal of Applied Chemistry
JF  - American Journal of Applied Chemistry
JO  - American Journal of Applied Chemistry
SP  - 54
EP  - 59
PB  - Science Publishing Group
SN  - 2330-8745
UR  - https://doi.org/10.11648/j.ajac.s.2015030301.18
AB  - The present work reports slightly modification of the conventional chemical synthesis of polyaniline (PANI) to be nanotube structure without the need for any template or structural directing materials. PANI preparation was optimized by the oxidation of two different precursors: aniline and aniline hydrochloride with ammonium persulfate (APS) as oxidizing agent in various aqueous media of strong, weak acid and in alkaline medium at different pH values. Structural and morphological properties of the products are characterized by SEM, XRD and FTIR. Results showed the strong dependence of PANI nanotube on the acidity at certain pH value during the oxidation of aniline by APS. It is founded that, the optimum condition for preparation of PANI nanotube was obtained under oxidation of aniline monomer by APS in aqueous media of weak acid medium at pH five degree.
VL  - 3
IS  - 3-1
ER  -

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