Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination

Klouda Karel; Zemanova Eva; Friedrichova Romana; Weisheitova Marketa

doi:doi:10.11648/j.ijmsa.20140306.13

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Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination

Klouda Karel, Zemanova Eva, Friedrichova Romana, Weisheitova Marketa

Published in International Journal of Materials Science and Applications (Volume 3, Issue 6)

Received: 5 September 2014 Accepted: 23 September 2014 Published: 10 October 2014

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Abstract

A direct reaction with liquid bromine was used to prepare bromofullerene C60Br14-18. The brominated derivative reacted with previously prepared graphene-oxide (hereinafter GO), according to a method described by Hummer. The same method was used to oxidize graphite alone. The prepared graphite fullerene foil was brominated with liquid bromine and the graphene-oxide foil was reacted with bromofullerene. FT-IR analysis of all the obtained products was performed and also TGA analysis to investigate particularly their thermal stability. The brominated products demonstrate lower thermal effects when thermally decomposed which is caused by the retarding ability of bromine.

Published in	International Journal of Materials Science and Applications (Volume 3, Issue 6)
DOI	10.11648/j.ijmsa.20140306.13
Page(s)	293-302
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2014. Published by Science Publishing Group

Keywords

Liquid Bromine, Graphene-Oxide Foil, Graphene-Oxide Foil with Fullerene, Brominated Fullerene, Fullerene C60

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APA Style

Klouda Karel, Zemanova Eva, Friedrichova Romana, Weisheitova Marketa. (2014). Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination. International Journal of Materials Science and Applications, 3(6), 293-302. https://doi.org/10.11648/j.ijmsa.20140306.13

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ACS Style

Klouda Karel; Zemanova Eva; Friedrichova Romana; Weisheitova Marketa. Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination. Int. J. Mater. Sci. Appl. 2014, 3(6), 293-302. doi: 10.11648/j.ijmsa.20140306.13

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AMA Style

Klouda Karel, Zemanova Eva, Friedrichova Romana, Weisheitova Marketa. Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination. Int J Mater Sci Appl. 2014;3(6):293-302. doi: 10.11648/j.ijmsa.20140306.13

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@article{10.11648/j.ijmsa.20140306.13,
  author = {Klouda Karel and Zemanova Eva and Friedrichova Romana and Weisheitova Marketa},
  title = {Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination},
  journal = {International Journal of Materials Science and Applications},
  volume = {3},
  number = {6},
  pages = {293-302},
  doi = {10.11648/j.ijmsa.20140306.13},
  url = {https://doi.org/10.11648/j.ijmsa.20140306.13},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20140306.13},
  abstract = {A direct reaction with liquid bromine was used to prepare bromofullerene C60Br14-18. The brominated derivative reacted with previously prepared graphene-oxide (hereinafter GO), according to a method described by Hummer. The same method was used to oxidize graphite alone. The prepared graphite fullerene foil was brominated with liquid bromine and the graphene-oxide foil was reacted with bromofullerene. FT-IR analysis of all the obtained products was performed and also TGA analysis to investigate particularly their thermal stability. The brominated products demonstrate lower thermal effects when thermally decomposed which is caused by the retarding ability of bromine.},
 year = {2014}
}

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TY  - JOUR
T1  - Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination
AU  - Klouda Karel
AU  - Zemanova Eva
AU  - Friedrichova Romana
AU  - Weisheitova Marketa
Y1  - 2014/10/10
PY  - 2014
N1  - https://doi.org/10.11648/j.ijmsa.20140306.13
DO  - 10.11648/j.ijmsa.20140306.13
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 293
EP  - 302
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20140306.13
AB  - A direct reaction with liquid bromine was used to prepare bromofullerene C60Br14-18. The brominated derivative reacted with previously prepared graphene-oxide (hereinafter GO), according to a method described by Hummer. The same method was used to oxidize graphite alone. The prepared graphite fullerene foil was brominated with liquid bromine and the graphene-oxide foil was reacted with bromofullerene. FT-IR analysis of all the obtained products was performed and also TGA analysis to investigate particularly their thermal stability. The brominated products demonstrate lower thermal effects when thermally decomposed which is caused by the retarding ability of bromine.
VL  - 3
IS  - 6
ER  -

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Author Information

Klouda Karel

V?B-Technical University of Ostrava, Faculty of Safety Engineering, Ostrava, CZ
Zemanova Eva

State Office for Nuclear Safety, Prague, CZ
Friedrichova Romana

Ministry of the Interior – General Directorate of the Fire Rescue Service of the Czech Republic, Technical Institute of Fire Protection, Prague, CZ
Weisheitova Marketa

National Institute for Nuclear, Chemical and Biological Protection, Kamenna, CZ

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APA Style

Klouda Karel, Zemanova Eva, Friedrichova Romana, Weisheitova Marketa. (2014). Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination. International Journal of Materials Science and Applications, 3(6), 293-302. https://doi.org/10.11648/j.ijmsa.20140306.13

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ACS Style

Klouda Karel; Zemanova Eva; Friedrichova Romana; Weisheitova Marketa. Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination. Int. J. Mater. Sci. Appl. 2014, 3(6), 293-302. doi: 10.11648/j.ijmsa.20140306.13

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AMA Style

Klouda Karel, Zemanova Eva, Friedrichova Romana, Weisheitova Marketa. Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination. Int J Mater Sci Appl. 2014;3(6):293-302. doi: 10.11648/j.ijmsa.20140306.13

Copy | Download

@article{10.11648/j.ijmsa.20140306.13,
  author = {Klouda Karel and Zemanova Eva and Friedrichova Romana and Weisheitova Marketa},
  title = {Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination},
  journal = {International Journal of Materials Science and Applications},
  volume = {3},
  number = {6},
  pages = {293-302},
  doi = {10.11648/j.ijmsa.20140306.13},
  url = {https://doi.org/10.11648/j.ijmsa.20140306.13},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20140306.13},
  abstract = {A direct reaction with liquid bromine was used to prepare bromofullerene C60Br14-18. The brominated derivative reacted with previously prepared graphene-oxide (hereinafter GO), according to a method described by Hummer. The same method was used to oxidize graphite alone. The prepared graphite fullerene foil was brominated with liquid bromine and the graphene-oxide foil was reacted with bromofullerene. FT-IR analysis of all the obtained products was performed and also TGA analysis to investigate particularly their thermal stability. The brominated products demonstrate lower thermal effects when thermally decomposed which is caused by the retarding ability of bromine.},
 year = {2014}
}

Copy | Download

TY  - JOUR
T1  - Fullerene C60, Graphene-Oxide and Graphene-Oxide Foil with Fullerene and their Bromination
AU  - Klouda Karel
AU  - Zemanova Eva
AU  - Friedrichova Romana
AU  - Weisheitova Marketa
Y1  - 2014/10/10
PY  - 2014
N1  - https://doi.org/10.11648/j.ijmsa.20140306.13
DO  - 10.11648/j.ijmsa.20140306.13
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 293
EP  - 302
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20140306.13
AB  - A direct reaction with liquid bromine was used to prepare bromofullerene C60Br14-18. The brominated derivative reacted with previously prepared graphene-oxide (hereinafter GO), according to a method described by Hummer. The same method was used to oxidize graphite alone. The prepared graphite fullerene foil was brominated with liquid bromine and the graphene-oxide foil was reacted with bromofullerene. FT-IR analysis of all the obtained products was performed and also TGA analysis to investigate particularly their thermal stability. The brominated products demonstrate lower thermal effects when thermally decomposed which is caused by the retarding ability of bromine.
VL  - 3
IS  - 6
ER  -

Copy | Download